- AutorIn
- Thomas Meier
- Tobias Herzig
- Jürgen Haase
- Titel
- Moissanite anvil cell design for giga-pascal nuclear magnetic resonance
- Zitierfähige Url:
- https://nbn-resolving.org/urn:nbn:de:bsz:15-qucosa2-213116
- Quellenangabe
- Review of Scientific Instruments Verlag: AIP Publishing
Erscheinungsjahr: 2014
Jahrgang: 85
Heft: 4
Artikelnummer: 043903 - Erstveröffentlichung
- 2014
- Abstract (EN)
- A new design of a non-magnetic high-pressure anvil cell for nuclear magnetic resonance (NMR) experiments at Giga-Pascal pressures is presented, which uses a micro-coil inside the pressurized region for high-sensitivity NMR. The comparably small cell has a length of 22 mm and a diameter of 18 mm, so it can be used with most NMR magnets. The performance of the cell is demonstrated with externalforce vs. internal-pressure experiments, and the cell is shown to perform well at pressures up to 23.5 GPa using 800 μm 6H-SiC large cone Boehler-type anvils. 1H, 23Na, 27Al, 69Ga, and 71Ga NMR test measurements are presented, which show a resolution of better than 4.5 ppm, and an almost maximum possible signal-to-noise ratio.
- Andere Ausgabe
- Link zur Originalpublikation in Review of Scientific Instruments
Link: https://dx.doi.org/10.1063/1.4870798 - Freie Schlagwörter (EN)
- Moissanite anvil cell design, nuclear magnetic resonance, NMR
- Klassifikation (DDC)
- 543.66
- Verlag
- AIP Publishing, Melville
- Version / Begutachtungsstatus
- publizierte Version / Verlagsversion
- URN Qucosa
- urn:nbn:de:bsz:15-qucosa2-213116
- Veröffentlichungsdatum Qucosa
- 28.05.2018
- Dokumenttyp
- Artikel
- Sprache des Dokumentes
- Englisch