Summary
Open tubular columns made of soda glass may be successfully coated with polar stationary phases after etching with dry HCl. Such columns are useful in difficult separations of steroids and their subsequent identification.
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References
K. Grob, Helv. Chim. Acta48, 1362 (1968).
M. Novotný andA. Zlatkis, Chromat. Reviews14, 1 (1971).
J. A. Völlmin, Chromatographia3, 233 (1970).
J. A.Völlmin, Clin. Chim. Acta34, 207 (1971).
H. Groenendijk, Doctoral Thesis, Eindhoven University of Technology (1971).
G. A. F. M. Rutten andJ. A. Luyten, J. Chromatog., to be published December 1972.
K. Grob, Helv. Chim. Acta51, 718, (1968).
K. Tesařîk andM. Novotný, in Gas-Chromatographie 1968: Vorträge des VI. Symposiums über Gas-Chromatographie, ed.H. G. Struppe, Berlin.
C. Hishta andJ. Bomstein, Advan. in Chromat.9, 215 (1970).
J. Bouche andM. Verzele, J. of Gas Chromat.6, 501 (1968).
H. Ch. Curtius andM. Müller, J. of Chromat.30, 410 (1967).
R. Kaiser, Chromatographie in der Gasphase, 2. Auflage, Band II, Bibliographisches Institut, Mannheim 1966.
L. S. Ettre, Open Hole Tubular Columns in Gas Chromatography, Plenum Press, New York 1965.
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Alexander, G., Rutten, G.A.F.M. Preparation of polar phase coated open tubular columns for steroid analysis. Chromatographia 6, 231–233 (1973). https://doi.org/10.1007/BF02311732
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DOI: https://doi.org/10.1007/BF02311732