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Poly(vinyl pyrrolidone)-assisted hydrothermal synthesis of Pb(Zr0.52Ti0.48)O3 nanocrystals

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Abstract

Pb(Zr0.52Ti0.48)O3 nanocrystals were synthesized by a hydrothermal method. The poly(vinyl pyrrolidone) (PVP) was used as the surfactant to control growth of the Pb(Zr0.52Ti0.48)O3 nanocrystals. The effect of PVP concentration, reaction temperature and time on morphologies and crystallinity of Pb(Zr0.52Ti0.48)O3 nanocrystals were investigated. The tetragonal PbZr0.52Ti0.48O3 grains were obtained, as they were prepared at 200 °C for 4 h with PVP concentration from 0.1 to 10.0 g/L. With increasing the PVP concentration from 0.1 to 10.0 g/L, the size of PbZr0.52Ti0.48O3 grains decreased. When the PbZr0.52Ti0.48O3 grains were prepared at 200 °C for 12 h with PVP concentration of 6.0 g/L, the PbZr0.52Ti0.48O3 nanocrystals with average diameter of 30 nm were formed.

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Acknowledgements

This work was financially supported by 111 project of China (Grant No. B13035) and the Fundamental Research Funds for the Central Universities (WUT: 2016III020).

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Authors and Affiliations

  1. School of Materials Science and Engineering, Wuhan University of Technology, Wuhan, 430070, China

    Xinyi Li, Qin Ma, Zhixiong Huang, Lianmeng Zhang & Dongyun Guo

  2. Department of Mechanical Science and Engineering, Nagoya University, Nagoya, 464-8603, Japan

    Yang Ju

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  1. Xinyi Li
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  2. Qin Ma
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Correspondence to Dongyun Guo.

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Li, X., Ma, Q., Huang, Z. et al. Poly(vinyl pyrrolidone)-assisted hydrothermal synthesis of Pb(Zr0.52Ti0.48)O3 nanocrystals. J Mater Sci: Mater Electron 30, 17164–17169 (2019). https://doi.org/10.1007/s10854-019-02063-9

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